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Beilstein J. Org. Chem. 2016, 12, 1334–1339, doi:10.3762/bjoc.12.126
Graphical Abstract
Figure 1: Previously reported PNHC complexes of interest for this work, along with the targeted complex 5.
Figure 2: Crystal structure of 6-Pd. The atoms of the tert-butyl groups, C–H bonds, and the solvent have been...
Scheme 1: Formation of dimers 6-Pd and 6-Pt by addition of NaOt-Bu.
Scheme 2: Formation of 7 and 8 by addition of LiN(iPr)2 (1 or 2 equiv) (R = tert-butyl).